Full Report Set



  ASAP 2020 V3.01 H    Unit 1    Serial #: 220    Page  1  

     Sample:    SJO-063                  
   Operator:                             
  Submitter:                             
       File:    D:\DATA\PAT\SJO-063.SMP  

            Started:    03.02.2021 10:57:07       Analysis Adsorptive:    N2                    
          Completed:    04.02.2021 16:10:26       Analysis Bath Temp.:    -195.831 C           
        Report Time:    04.02.2021 18:04:13        Thermal Correction:    No                    
        Sample Mass:    0.0415 g                      Warm Free Space:    16.2606 cm Measured  
    Cold Free Space:    49.1066 cm            Equilibration Interval:    45 s                  
  Low Pressure Dose:    0.5000 mmol/g                 Automatic Degas:    Yes                   







                      Isotherm Tabular Report

   Relative       Absolute      Quantity    Elapsed    Saturation   
   Pressure       Pressure      Adsorbed     Time       Pressure    
    (p/p)          (kPa)       (mmol/g)    (h:min)       (kPa)     
-----
  1.#QNAN0000      1.#QNAN00     1.#QNAN      00:59    100.2079688  
  0.000010002      0.0010023     0.51235      01:58      1.#QNAN00  
  0.000005502      0.0005514     1.02595      02:49      1.#QNAN00  
  0.000008555      0.0008574     1.53821      03:42      1.#QNAN00  
  0.000021539      0.0021588     2.04639      04:34      1.#QNAN00  
  0.000055664      0.0055793     2.54433      05:35      1.#QNAN00  
  0.000126808      0.0127111     3.02058      07:05      1.#QNAN00  
  0.000258758      0.0259410     3.45687      09:41      1.#QNAN00  
  0.000468652      0.0469889     3.82551      12:01      1.#QNAN00  
  0.001018192      0.1020942     4.30802      13:14      1.#QNAN00  
  0.001994922      0.2000445     4.76256      14:35      1.#QNAN00  
  0.003584455      0.3594643     5.19231      16:02      1.#QNAN00  
  0.005891591      0.5908680     5.58121      17:11      1.#QNAN00  
  1.#QNAN0000      1.#QNAN00     1.#QNAN      17:16    100.2904734  
  0.008779106      0.8807697     5.89601      17:30      1.#QNAN00  
  0.012659220      1.2702358     6.19957      17:36      1.#QNAN00  
  0.014303227      1.4353765     6.30805      17:41      1.#QNAN00  
  0.016038315      1.6097000     6.41172      17:46      1.#QNAN00  
  0.017155417      1.7220346     6.47977      17:51      1.#QNAN00  
  0.018555373      1.8627000     6.55003      17:54      1.#QNAN00  
  0.020729678      2.0811783     6.65539      17:58      1.#QNAN00  
  0.023646114      2.3743338     6.78629      18:04      1.#QNAN00  
  0.027045837      2.7160439     6.91766      18:09      1.#QNAN00  
  0.030153996      3.0284801     7.02844      18:13      1.#QNAN00  
  0.033983261      3.4134949     7.15248      18:18      1.#QNAN00  
  1.#QNAN0000      1.#QNAN00     1.#QNAN      18:20    100.4513896  
  0.034681379      3.4840532     7.18340      18:23      1.#QNAN00  
  0.040067966      4.0255849     7.33654      18:27      1.#QNAN00  
  0.044510841      4.4724014     7.45387      18:31      1.#QNAN00  
  0.051368164      5.1619322     7.61387      18:35      1.#QNAN00  
  0.052201035      5.2460186     7.63592      18:38      1.#QNAN00  
  0.052475439      5.2739892     7.65204      18:41      1.#QNAN00  
  0.053727437      5.4002234     7.68039      18:44      1.#QNAN00  
  0.054915402      5.5200399     7.70858      18:47      1.#QNAN00  
  0.055319923      5.5609789     7.72118      18:49      1.#QNAN00  
  0.056988080      5.7290966     7.75855      18:52      1.#QNAN00  
  0.058309981      5.8624272     7.78751      18:55      1.#QNAN00  
  0.059766070      6.0092698     7.81968      18:58      1.#QNAN00  
  0.061388340      6.1728443     7.85172      19:01      1.#QNAN00  
  0.063233387      6.3586877     7.88957      19:03      1.#QNAN00  
  0.064986106      6.5354275     7.92105      19:06      1.#QNAN00  
  0.066950899      6.7335227     7.96182      19:09      1.#QNAN00  
  0.068871939      6.9270742     7.99702      19:11      1.#QNAN00  
  0.071011349      7.1427874     8.03354      19:14      1.#QNAN00  
  0.073173546      7.3606416     8.07226      19:16      1.#QNAN00  
  0.075256088      7.5708813     8.11322      19:20      1.#QNAN00  
  1.#QNAN0000      1.#QNAN00     1.#QNAN      19:22    100.6065852  
  0.080073121      8.0564723     8.19468      19:25      1.#QNAN00  
  0.085897608      8.6431287     8.28699      19:28      1.#QNAN00  
  0.097589860      9.8205753     8.45736      19:32      1.#QNAN00  
  0.100032369     10.0671035     8.49432      19:35      1.#QNAN00  
  0.111099920     11.1817419     8.64237      19:38      1.#QNAN00  
  0.126574699     12.7404550     8.82843      19:42      1.#QNAN00  
  0.140623250     14.1555551     8.98843      19:45      1.#QNAN00  
  0.143696688     14.4656411     9.02805      19:47      1.#QNAN00  
  0.163925024     16.5035925     9.23339      19:51      1.#QNAN00  
  0.186992661     18.8273643     9.45908      19:54      1.#QNAN00  
  0.212655845     21.4128273     9.69374      19:57      1.#QNAN00  
  0.241862987     24.3561366     9.94598      20:01      1.#QNAN00  
  0.251258304     25.3041139    10.03193      20:04      1.#QNAN00  
  0.275730830     27.7707593    10.23149      20:07      1.#QNAN00  
  0.300987649     30.3167623    10.43853      20:10      1.#QNAN00  
  0.313700772     31.5988206    10.54477      20:12      1.#QNAN00  
  0.350218093     35.2806151    10.82050      20:16      1.#QNAN00  
  0.354300866     35.6936468    10.86518      20:18      1.#QNAN00  
  0.400372265     40.3389852    11.21975      20:22      1.#QNAN00  
  1.#QNAN0000      1.#QNAN00     1.#QNAN      20:24    100.7585991  
  0.421411142     42.4639656    11.39687      20:27      1.#QNAN00  
  0.450646661     45.4133046    11.62486      20:30      1.#QNAN00  
  0.459679489     46.3258803    11.70616      20:32      1.#QNAN00  
  0.500292605     50.4225781    12.03662      20:35      1.#QNAN00  
  0.522845069     52.6994869    12.23517      20:38      1.#QNAN00  
  0.550254039     55.4662766    12.47783      20:41      1.#QNAN00  
  0.594970826     59.9797492    12.89282      20:45      1.#QNAN00  
  0.600007778     60.4905390    12.96301      20:47      1.#QNAN00  
  0.650779101     65.6156396    13.48977      20:51      1.#QNAN00  
  0.675451632     68.1083592    13.79363      20:54      1.#QNAN00  
  0.699921813     70.5810446    14.11955      20:57      1.#QNAN00  
  0.738864759     74.5155119    14.69259      21:01      1.#QNAN00  
  0.772768838     77.9444707    15.28970      21:06      1.#QNAN00  
  0.806612584     81.3661709    16.01418      21:10      1.#QNAN00  
  0.876097097     88.3995052    18.22809      21:21      1.#QNAN00  
  0.912655586     92.1066149    20.25563      21:29      1.#QNAN00  
  1.#QNAN0000      1.#QNAN00     1.#QNAN      21:31    100.9265622  
  0.926292456     93.5016910    21.42902      21:38      1.#QNAN00  
  0.946227107     95.5346216    23.85115      21:48      1.#QNAN00  
  0.953867589     96.3206330    25.21607      21:55      1.#QNAN00  
  0.981619961     99.1702609    35.90446      22:17      1.#QNAN00  
  1.#QNAN0000      1.#QNAN00     1.#QNAN      22:39    101.0752479  
  0.990920414    100.1807168    46.85174      22:49      1.#QNAN00  
  0.984130242     99.5103616    45.41004      22:56      1.#QNAN00  
  0.979986947     99.1097597    43.13539      23:04      1.#QNAN00  
  0.976357163     98.7632305    40.91717      23:13      1.#QNAN00  
  0.971899235     98.3350348    38.05221      23:23      1.#QNAN00  
  0.967349454     97.8973347    35.40444      23:33      1.#QNAN00  
  0.962564723     97.4378916    33.04363      23:44      1.#QNAN00  
  1.#QNAN0000      1.#QNAN00     1.#QNAN      23:46    101.2320466  
  0.957623551     96.9557371    30.89923      23:56      1.#QNAN00  
  0.952423971     96.4414238    29.14536      24:05      1.#QNAN00  
  0.947403329     95.9437596    27.72933      24:13      1.#QNAN00  
  0.939427027     95.1492853    25.97707      24:23      1.#QNAN00  
  0.933347843     94.5428002    24.86303      24:30      1.#QNAN00  
  0.924472843     93.6542745    23.55489      24:38      1.#QNAN00  
  0.914779881     92.6826745    22.38731      24:46      1.#QNAN00  
  1.#QNAN0000      1.#QNAN00     1.#QNAN      24:48    101.3197429  
  0.904457345     91.6448934    21.38740      24:55      1.#QNAN00  
  0.890033564     90.1888116    20.32950      25:02      1.#QNAN00  
  0.876009531     88.7723018    19.48405      25:08      1.#QNAN00  
  0.860316631     87.1865187    18.68377      25:14      1.#QNAN00  
  0.839504575     85.0810273    17.89017      25:19      1.#QNAN00  
  0.821229663     83.2324973    17.29223      25:24      1.#QNAN00  
  0.799755987     81.0595961    16.72260      25:29      1.#QNAN00  
  0.770429212     78.0905199    16.07700      25:34      1.#QNAN00  
  0.740143148     75.0233072    15.52443      25:38      1.#QNAN00  
  0.700150859     70.9719956    14.92116      25:42      1.#QNAN00  
  0.650381620     65.9293142    14.28971      25:46      1.#QNAN00  
  0.600184582     60.8429190    13.75125      25:50      1.#QNAN00  
  1.#QNAN0000      1.#QNAN00     1.#QNAN      25:52    101.3754186  
  0.550425524     55.8015762    13.26761      25:56      1.#QNAN00  
  0.500368995     50.7286768    12.81523      26:00      1.#QNAN00  
  0.452376646     45.8651027    12.19062      26:05      1.#QNAN00  
  0.396323163     40.1834194    11.69511      26:09      1.#QNAN00  
  0.351960747     35.6867422    11.35372      26:13      1.#QNAN00  
  0.300854617     30.5056852    10.96035      26:16      1.#QNAN00  
  0.250395058     25.3901399    10.55569      26:20      1.#QNAN00  
  0.200486103     20.3300690    10.11606      26:24      1.#QNAN00  
  0.150441802     15.2560518     9.60934      26:29      1.#QNAN00  
  0.100747974     10.2173109     8.98846      26:36      1.#QNAN00  
  0.070377442      7.1376725     8.47632      26:42      1.#QNAN00  

       
 Options Report


              Sample Tube

         Warm freespace:    1.0000 cm  
         Cold freespace:    1.0000 cm  
    Non-ideality factor:    0.0000620   
  Use Isothermal Jacket:    Yes         
         Use Filler Rod:    Yes         
       Vacuum seal type:    Seal Frit   

 Analysis Conditions


                 Preparation

               Fast evacuation:    No        
  Unrestricted evacuation from:    0.67 kPa  
               Vacuum setpoint:    1.3 Pa    
               Evacuation time:    0.10 h    
                     Leak test:    No        
                 Use TransSeal:    No        

                Free Space

             Free-space type:    Measured  
  Lower dewar for evacuation:    Yes       
             Evacuation time:    0.10 h    
                 Outgas test:    No        

                                                       p and Temperature

         p and T type:    Measure p at intervals during analysis.  Calculate the Analysis Bath Temperature from these values.  
  Measurement interval:    60 min                                                                                                

                         Dosing

  Use first pressure fixed dose:    No                  
   Use maximum volume increment:    No                  
               Target tolerance:    5.0% or 0.6666 kPa  
            Low pressure dosing:    Yes                 
                    Dose amount:    0.50000 mmol/g      
    Minimum equilibration delay:    0.00 h              
    Maximum equilibration delay:    999.00 h            

                      Equilibration

       Equilibration time (p/p = 0.010000000):    45 s   
       Equilibration time (p/p = 1.000000000):    10 s   
  Minimum equilibration delay at p/p >= 0.995:    600 s  

             Sample Backfill

  Backfill at start of analysis:    Yes  
    Backfill at end of analysis:    Yes  
                   Backfill gas:    N2   

                Adsorptive Properties

                         Adsorptive:    Nitrogen     
          Maximum manifold pressure:    123.323 kPa  
                Non-ideality factor:    0.0000620    
          Density conversion factor:    0.0015468    
  Therm. tran. hard-sphere diameter:    3.860       
     Molecular cross-sectional area:    0.162 nm    


  Inside diameter of sample tube:    9.53 mm  

